ASTM D5765-2005 用封闭式容器微波加热法从土壤和沉积物中溶剂萃取全部石油烃类的标准实施规程

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【英文标准名称】:StandardPracticeforSolventExtractionofTotalPetroleumHydrocarbonsfromSoilsandSedimentsUsingClosedVesselMicrowaveHeating
【原文标准名称】:用封闭式容器微波加热法从土壤和沉积物中溶剂萃取全部石油烃类的标准实施规程
【标准号】:ASTMD5765-2005
【标准状态】:现行
【国别】:
【发布日期】:2005
【实施或试行日期】:
【发布单位】:美国材料与试验协会(US-ASTM)
【起草单位】:D19.07
【标准类型】:(Practice)
【标准水平】:()
【中文主题词】:规程;溶剂萃取方法;实施规程;加热试验;沉积物;烃类;土壤普查;土壤;微波灶
【英文主题词】:extraction;microwave;solvent;totalpetroleumhydrocarbon(TPH);vessel
【摘要】:Solventextractionofsoilsandsedimentscanprovideinformationontheavailabilityofpetroleumhydrocarbonstoleaching,waterqualitychanges,orothersiteconditions.Rapidheating,incombinationwithtemperaturesinexcessoftheatmosphericboilingpointofacetone/hexane,reducessamplepreparationorextractiontimes.Reducedamountsofsolventsarerequiredandsolventlossduetoboilingandevaporationareeliminatedbyuseofclosedextractionvessels.1.1Thispracticecoversthesolventextractionoftotalpetroleumhydrocarbon(TPH)fromsoilsandsediments,usingclosedvesselmicrowaveheating,forsubsequentdeterminationbygravimetricorgaschromatographictechniques.1.2Thispracticeisrecommendedonlyforsolidsamplesthatcanpassthroughatenmeshscreen(approximately2-mmopenings).1.3Thesolventextractobtainedbythispracticemaybeanalyzedfortotalorspecificnonvolatileandsemivolatilepetroleumhydrocarbonsbutmayrequiresampleclean-upprocedurespriortospecificcompoundanalysis.1.4Thispracticeislimitedtosolventsthatarerecommendedforuseinmicrowavesolventextractionsystems.1.5Thevaluesstatedinpoundspersquareinch(psi)aretoberegardedasthestandard.TheSIunitsgiveninparenthesesareforinformationonly.1.6Thisstandarddoesnotpurporttoaddressallofthesafetyconcerns,ifany,associatedwithitsuse.Itistheresponsibilityoftheuserofthisstandardtoestablishappropriatesafetyandhealthpracticesanddeterminetheapplicabilityofregulatorylimitationspriortouse.SpecifichazardstatementsaregiveninSection8.
【中国标准分类号】:E04
【国际标准分类号】:13_080_10
【页数】:3P.;A4
【正文语种】: